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  2. Successful Completion of a Research Degree: Guidelines for…

    https://www.ch.cam.ac.uk/gradstudents/files/Postgraduate%20Education%20Files/Guidelines%20for%20Experimentalists%202023-24%20V1.0.pdf
    9 May 2024: Purification by flash column chromatography (20% EtOAc in hexane) afforded 9 (4.56 g, 92%, 50:50 mixture of diastereomers by 1H NMR) as a colorless oil. ... The crude product was purified using silica gel flash chromatography eluting with 3-5%

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